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1 article(s) from Friedrich, Steffen

Synthesis of complex intermediates for the study of a dehydratase from borrelidin biosynthesis

Frank Hahn,
Nadine Kandziora,
Steffen Friedrich and
Peter F. Leadlay

Beilstein J. Org. Chem. 2014, 10, 634–640, doi:10.3762/bjoc.10.55

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Figure 1: a) Structure of borrelidin (1); b) PKS intermediates are attached to an acyl carrier protein domain...

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Scheme 1: Retrosynthetic analysis of surrogate substrates for BorDH3 and reference molecules for enzyme assay...

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Scheme 2: Synthesis of the common precursor aldehyde 11. Compound 13 was prepared in six steps and with an ov...

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Scheme 3: Synthesis of the BorDH3 substrates. a) Thiophenolpropionate, Cy₂BCl, Me₂EtN, Et₂O, −78 °C to −20 °C...

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Scheme 4: Synthesis of reference compounds for the BorDH3 assay. a) 24, CH₂Cl₂, 50 °C, 3 h (88% over two step...

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Published 11 Mar 2014

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